下载中心
硅烷法固定ssDNA制作的压电式DNA传感器pdf
1星 发布者: jasionla

2013-09-20 | 1积分 | 199.95KB |  0 次下载

下载 收藏 评论

文档简介
标签: 硅烷法固定ssDNA制作的压电式DNA传感器

硅烷法固定ssDNA制作的压电式DNA传感器

利用硅烷法将ssDNA 固化T方向切割、3. 58MHz 和10MHz 石英晶体金电极上,构建了压电DNA传感器,建立了快速检测葡萄球菌肠毒素B(SEB) 基因的方法。优化了固定SEB 基因的条件,并用动态法、静态法和斑点杂交法进行了固化效果观察。结果表明:该传感器2 h 后,有较好响应;对不同长度DNA 探针固化效果进行比较,169 bp (即169 个碱基) SEB 探针固定和杂交效果较好;利用0. 5mol/ LNaOH进行电极洗脱,时间为45min ,电极可以再生,且传感器可以重复使用3 次;利用1. 2mol/ L NaOH和1. 2mol/ L HCl洗涤电极,该电极可多次再利用;固化好的电极于4 ℃条件下可以保存三周之久。关键词: 压电式DNA 传感器; 葡萄球菌肠毒素B ; 3 - 氨基丙基三乙氧基甲硅烷Abstract : A rapid method has been developed to monitor Staphylococcal enterotoxin B(SEB) gene by using piezoeletric DNA sensor system. AT2cut crystals ,with a based resonant frequency of 3. 58MHz and 10MHz ,were modified by 32 aminopropyltriethoxysilane(32APTES) treatment and then single stranded SEB gene probe was electro2blotted onto thesurface of crystal electrodes. The optimization condition of immobilization for piezoeletric DNA sensor was researched. Im2 mobililzed efficiency was observed by active methods , passive methods and dot hybridization method. There is better re2 sponse of the piezoelectric DNA sensor after DNA hybridization for 2 h. Hybridization effect of 169 bp SEB gene probe was better comparing with the other different length of SEB gene probe. The sensor could be repeatedly used ,the complemen2 tary ssDNA of the SEB DNA probe could be removed from the crystal by washing with 0. 5mol/ L NaOH denaturant. After the hybridized electrode was immersed in 1. 2mol/ L NaOH and then 1. 2 mol/ L HCl ,all substances could be removedfrom the crystal surface ,and the quartz crystal could be reused for many times. The 32APTES2coated ssDNA electrode was stable for over three weeks when stored at 4 ℃.Key words : piezoelectric DNA sensor ; staphylococcal enterotoxin B (SEB) ; 32aminopropyltriethoxysilane (32APTES)

评论
相关视频
  • 财哥说钛丝

  • 直播回放: Keysight 小探头,大学问,别让探头拖累你的测试结果!

  • 控制系统仿真与CAD

  • MIT 6.622 Power Electronics

  • 直播回放:基于英飞凌AIROC™ CYW20829低功耗蓝牙芯片的无线组网解决方案

  • 直播回放:ADI & WT·世健MCU痛点问题探索季:MCU应用难题全力击破!

推荐帖子
精选电路图
  • CCD图像传感器在微光电视系统中的应用

  • 如何利用ESP8266制作一个简单的四轴飞行器

  • 非常简单的150W功放电路图

  • 一个简单的警笛电路图

  • 优化电路板布局的简单方法

  • 使用NE555和磁簧开关的橱柜照明电路

×